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Article Abstracts

Published:Journal of Chromatographic Science, ISSN 0021-9665Volume 39, Number 6, June 2001, pp. 255-259

Collaborative Study of EPA Method 317.0 for the Determination of Inorganic Oxyhalide Disinfection By-Products in Drinking Water Using Ion Chromatography with the Addition of a Postcolumn Reagent for Trace Bromate Analysis Herbert P. Wagner[1], Barry V. Pepich[1], Christopher P. Frebis[2], Daniel P. Hautman[2], David J. Munch[2], and Peter E. Jackson[3]
[1] IT Corporation, Technology Applications Group, 26 W. Martin Luther King Drive, Cincinnati, OH 45219;
[2] U.S. Environmental Protection Agency, Office of Ground Water and Drinking Water, 26 W. Martin Luther King Drive, Cincinnati, OH 45268; and
[3] Dionex Corporation, 1228 Titan Way, Sunnyvale, CA 94088-3606

The development of the U.S. Environmental Protection Agency (EPA) Method 317.0 is initiated to provide a sufficiently sensitive and fundamental technique for the compliance monitoring of trace levels of bromate in drinking water. After a comparative evaluation of Method 317.0 and elimination of a chlorite interference, this method is tested by a collaborative study in order to determine the precision and bias of the method and evaluate its potential role as a future compliance-monitoring method for inorganic disinfection by-products (DBPs) and trace bromate. This technique provides a practical method for future compliance monitoring for all of the inorganic oxyhalide DBPs including trace concentrations of bromate.

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