Published: Journal of Chromatographic Science, Volume
37, Number 9, September 1999, pp. 323-329
Automated Solid-Phase Microextraction– Gas Chromatography–Mass
Selective Detection Investigations of Carbonyl–Amine Reaction Pathways
W.M. Coleman, III
Employing automated solid-phase microextraction– gas chromatography–selected
ion monitoring-mass selective detection, mechanistic information on the formation
of volatile components associated with carbonyl–amine chemistries in microwave
heat-treated natural products is gathered. Employing 13C uniformly labeled amino
acids and sugars, pathways for the formation of Strecker aldehydes, pyrazines,
and furan derivatives are delineated in a heat treated licorice suspension. The
results are among the first pieces of information providing unambiguous reaction
pathways for the production of these compounds in heated natural products.
Reproduction of editorial content
of this journal is prohibited without publisher’s
permission.
This article is available in its entirety by fax for $4.00 per page.
Visa or MasterCard accepted.
To order electronically
click here
or call: 847-647-2900 ext. 1323
or fax request to: 847-647-1155.
Please indicate JCS
volume and issue along with page numbers.
|
| Home
| Subscribe | Current Issue
| Back Issues | Search | Advertise | Other Publications
| Site Map |